Standardize a titrant before a QC assay
Practice the sequence you already learned for “Standardize a titrant before a QC assay” until the order feels automatic. Drill USP <541> titrant-standardization order. Sample assays are not started until the primary standard is dried, replicates are titrated, and the factor is within the method limit.
- Dry the required primary standard as the method says.
- Weigh the primary standard.
- Titrate the replicates specified.
- Calculate the normality or molarity factor.
- Compare to the previous factor and the limit.
- Label the bottle with the new factor and date.
- Do not use an expired factor because ‘it is close enough.’